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期刊信息

期刊名称:《中国胶粘剂》CHINA ADHESIVES

创办日期:1986(1973)

主管部门:上海华谊(集团)有限公司

主办单位:上海市合成树脂研究所有限公司、中国胶粘剂和胶粘带工业协会

刊 期:月刊     

电 话:010-87663098/87663304

Email:GXLJ@chinajournal.net.cn

国内统一刊号(CN):

CN 31-1601/TQ

国际标准刊号(ISSN):

ISSN 1004-2849

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本刊介绍

《中国胶粘剂》为重点报道中国胶粘剂科研成果和最新进展的学术期刊,月刊。1973年创刊,原名为《树脂粘合剂》,1979年更名为《粘合剂》,1991年更名为《中国胶粘剂》,201412月,成为原国家新闻出版广电总局第一批认定学术期刊。

主管单位是上海华谊控股集团有限公司,主办单位是上海市合成树脂研究所有限公司、中国胶粘剂和胶粘带工业协会。

期刊在国内外公开发行,国内发行代号为4-454,国外发行代号为M5121;国内统一连续出版物号为CN31-1601/TQ,国际标准连续出版物号为ISSN 1004-2849

期刊设有专题综述、研究报告、工艺与应用、材料科学等栏目,主要报道国内外胶粘剂、密封剂和胶粘带行业的最新理论研究成果、原料/设备/制备工艺创新、粘接接头设计制备技术、生产应用实践等论文和综述等,主要涉及领域主要包括化工、轻工、包装、纺织、建筑、机械、电子、航空、航天、汽车、船舶、林木、家具和印刷等领域。

期刊为中国科技核心期刊、RCCSE中国核心学术期刊,《科技期刊世界影响力指数(WJCI)报告》收录期刊,曾为全国中文核心期刊(2007/2011/2014/2017年),现被“中国核心期刊数据库、”“中国期刊全文数据库”、“中国学术期刊综合评价数据库”、《中国学术期刊影响因子年报》统计源、美国《化学文摘》(CA)、中国知网数据库(CNKI)、万方数据库、维普数据库、新华网“学术中国”以及长江文库等收录,先后荣获《CAJ-CD规范》执行优秀期刊、全国石油和化工行业优秀期刊二等奖、全国石油和化工行业优秀期刊一等奖、华东地区优秀期刊奖、上海市科技期刊审读优秀奖、上海市期刊编校质量优秀奖、全国石油和化工学术期刊50强、全国石油和化工行业期刊100强、全国石油和化工学术期刊60强。2024年,期刊还被中国化工学会发布的首版《化工领域高质量科技期刊分级目录》入选为T3级期刊,标志着我刊已进入化工领域国内外重要、为学术界所认可的期刊队列。2024年期刊复合影响因子为1.595,综合影响因子为1.309。

《中国胶粘剂》杂志是胶粘剂行业的窗口,是胶粘剂企业的桥梁,是胶粘剂读者的纽带。

2025年06期
专题综述

高性能压敏胶粘剂的研究进展

Research progress of high performance pressure sensitive adhesive

邢文旭;刘彩召;张绪刚;孙明明;张斌; Xing Wenxu;Liu Caizhao;Zhang Xugang;Sun Mingming;Zhang Bin;

压敏胶粘剂作为一种重要功能粘接材料,广泛应用于电子、汽车和包装等领域。本文系统总结了不同种类压敏胶的研究进展,涵盖了丙烯酸酯、有机硅、天然橡胶、热熔型及聚氨酯类压敏胶的结构特性、性能改进和改性方法,分析了其分子结构与黏附性能之间的关系。同时,探讨了新型改性技术在压敏胶性能提升中的应用。最后,展望了压敏胶的未来发展趋势,重点关注可持续性、智能化及多功能化研究方向,希望对高性能压敏胶粘剂的设计开发提供理论基础和实践指导。

Pressure sensitive adhesive,as an important functional bonding material,is widely used in electronics,automotive,and packaging industries. The research progress of different types of pressure sensitive adhesive,covering the structural characteristics,performance improvement,and modification methods of acrylate,silicone,natural rubber,hot melt and polyurethane pressure sensitive adhesive was systematically summarized in this article,and the relationship between their molecular structures and adhesion properties was analyzed.At the same time,the application of new modification technologies in improving the performance of pressure sensitive adhesive was explored.Finally,the future development trends of pressure sensitive adhesive were discussed,with a focus on sustainability,intelligence,and multifunctionality research directions.It was hoped that this would provide theoretical basis and practical guidance for the design and development of high performance pressure sensitive adhesive.

2025 年 06 期 v.34 ;
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仿生智能黏附界面的研究现状

Research status of biomimetic intelligent adhesion interface

周建伟;姚燕生;阚宏林; Zhou Jianwei;Yao Yansheng;Kan Honglin;

智能黏附界面,尤其是按需切换黏附力的界面,在可穿戴设备、机器人和生物检测等领域展现出巨大的应用潜力。本文聚焦于三种代表性仿生对象——壁虎、树蛙和章鱼,利用JKR模型、毛细管湿黏附模型和吸力负压模型分别解释三者黏附机制,并系统剖析了仿生可切换黏附领域(如攀爬机器人、软夹具和可穿戴设备等)的多种仿生智能黏附界面以及研究现状。最后对仿生智能黏附界面的未来发展进行了展望。

The intelligent adhesion interface,especially the interface that switches adhesion force on demand,has shown great potential for applications in wearable devices,robots,and biological detection. Three representative biomimetic objects—gecko,tree frog,and octopus were focused in this article. The JKR model,capillary wet adhesion model,and suction negative-pressure model were used to explain the adhesion mechanisms of three objects,and the various biomimetic intelligent adhesion interfaces and research status in the field of biomimetic switchable adhesion(such as climbing robot,soft fixture,and wearable device) were systematically analyzed.Finally,the future development of biomimetic intelligent adhesion interface was discussed.

2025 年 06 期 v.34 ; 安徽省自然科学基金面上项目(1908085ME130); 安徽省农业物质技术装备揭榜挂帅暨农机补短板项目(KZ22023128)
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研究报告

片银/球银复配对导电胶性能的影响

Influence of the mixing of flake silver/sphere silver on the performance of electrically conductive adhesive

桑广艺;蒋超;龚文圣;来立锋;陶小乐;何永富; Sang Guangyi;Jiang Chao;Gong Wensheng;Lai Lifeng;Tao Xiaole;He Yongfu;

采用环氧树脂、环氧稀释剂、固化剂、固化促进剂、偶联剂、导电助剂以及3倍前述质量的银粉(不同片银/球银比例),制备了导电胶(ECA),并从流变性能、热物理性能、导电性能、导热性能、形貌以及粘接强度几个方面研究了微米片银/微米球银复配对ECA性能的影响。研究结果表明:(1)黏度和触变指数受球银的占比影响很大,球银占比越高,黏度越小,触变指数越小。片银对提高ECA触变性有明显影响,而球银能有效降低黏度。(2)随着球银比例增加,玻璃化转变温度(Tg)发生轻微变化,对Tg前的热膨胀系数(CTE-1)影响不大,对Tg后的热膨胀系数(CTE-2)则有明显的降低作用。(3)在银粉总含量不变的情况下,球银对体积电阻率的降低不利,但能明显提升ECA的热导率。(4)添加的银粉整体呈现出均匀分布的特征,且具有一定的随机性和无序性。随着球银含量的增加,其在片银平面方向的填充密度由疏松逐渐趋于致密,同时片银被球银遮蔽的程度也相应提高。随着球银比例的进一步增加,大量的球银填充于片银平面垂直方向的间隙中,有利于构建各向同性的高效导热网络。(5)球银相对片银具有更紧密的堆积效果,机械补强效果随着球银含量的提升而得到体现,并且在球银含量达到1/3时,出现最佳粘接强度。

An electrically conductive adhesive(ECA) was prepared by using epoxy resin,epoxy diluent,curing agent,curing accelerator,coupling agent,conductive additive,and three times of the aforementioned mass of silver powder(different ratios of flake silver/sphere silver).The influence of micro flake silver/micro sphere silver compounding on the performance of ECA was studied from several aspects of rheological properties,thermophysical properties,electrical conductivity,thermal conductivity,morphology,and bonding strength. The research results showed that,(1) The viscosity and thixotropy index were greatly affected by the proportion of sphere silver.The higher the proportion of sphere silver,the lower the viscosity and thixotropy index.Flake silver had a significant effect on improving ECA thixotropy,while sphere silver could effectively reduce viscosity.(2) As the proportion of sphere silver increased,the glass transition temperature(Tg) underwent a slight change,with little effect on the coefficient of thermal expansion(CTE-1) before Tg,but a significant decrease in the coefficient of thermal expansion(CTE-2) after Tg.(3) Under the condition of fixed total content of silver powder,sphere silver was not conducive to reducing the volume resistivity,but it could significantly improve the thermal conductivity of ECA.(4) The added silver powder exhibited a uniform distribution as a whole,and had a certain degree of randomness and disorder.As the content of sphere silver increased,its filling density in the direction of flake silver gradually became denser from loose,and the degree of shielding of flake silver by sphere silver also increased accordingly.As the proportion of sphere silver increased further,a large amount of sphere silver filled the gaps in the vertical direction of flake silver,which was beneficial for constructing an isotropic and efficient thermal conductivity network.(5) Sphere silver had a tighter stacking effect compared to flake silver,and the mechanical reinforcement effect was reflected with the increase of sphere silver content.The optimal bonding strength occurred when the sphere silver content reached 1/3.

2025 年 06 期 v.34 ; 浙江省科技厅“尖兵”“领雁”研发攻关计划项目(2023C01087)
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导电助剂与稀释剂类型对LED固晶胶性能的影响

Influence of conductive additive and diluent type on the properties of LED die attach adhesive

蒋超;桑广艺;宋琦;李龙发;龚文圣;陈丹;陶小乐;何丹薇; Jiang Chao;Sang Guangyi;Song Qi;Li Longfa;Gong Wensheng;Chen Dan;Tao Xiaole;He Danwei;

LED固晶胶的导电、导热以及耐热可靠性对于大功率LED的发光性能与长期可靠性至关重要。本文采用环氧树脂、稀释剂、固化剂、固化促进剂、偶联剂、导电助剂和银粉等制备了LED固晶胶,然后通过改变导电助剂、稀释剂的种类,制备了不同的样品(E0~E4、R1~R5)。考察了导电助剂种类对LED固晶胶黏度、体积电阻率及导热性能的影响,并探究了稀释剂种类对LED固晶胶的常温及高温芯片推力、芯片-镀银框架残胶率及耐湿热性能的影响。研究结果表明:(1)导电助剂的加入,能够显著降低固晶胶的黏度。当导电助剂为己二酸(二元羧酸),固晶胶体积电阻率显著降低,热导率明显提升;当导电助剂中同时包含羧基和羟基时,体积电阻率反而增加,热导率降低。(2)分子刚性强(R4)、交联密度高(R5)的稀释剂,高温推力和残胶率表现不佳;单官刚性较强的苯基稀释剂(R1),在常温/高温芯片推力及残胶率间取得优异的平衡性能;柔性较好的脂肪族二缩水甘油醚稀释剂(R2、R3),综合性能介于两者之间。(3)高温蒸煮湿热老化试验表明,稀释剂中疏水性较好的苯基基团有助于改善固晶胶的耐湿热性能。

The electrical conductivity,thermal conductivity,and heat resistance reliability of LED die attach adhesive are crucial for the luminescence performance and long-term reliability of high-power LED.LED die attach adhesive was prepared in this article by using epoxy resin,diluent,curing agent,curing accelerator,coupling agent,conductive additive,and silver powder.Then,different samples(E0-E4,R1-R5) were prepared by changing the types of conductive additive and diluent. The influence of conductive additive type on the viscosity,volume resistivity,and thermal conductivity of LED die attach adhesive was investigated,and the influence of diluent type on die shear force at the room temperature and high temperature,residual adhesive rate of chip-silver plating frame,and moisture and heat resistance of LED die attach adhesive were explored.The research results showed that,(1) The addition of conductive additive could significantly reduce the viscosity of die attach adhesive.When the conductive additive was adipic acid(dicarboxylic acid),the volume resistivity of die attach adhesive significantly decreased and the thermal conductivity significantly increased. When both carboxyl and hydroxyl groups were present in the conductive additive,the volume resistivity increased,while the thermal conductivity decreased.(2) For diluents with strong molecular rigidity(R4) and high crosslinking density(R5),they exhibited poor performance in high-temperature die shear force and residual adhesive rate.For phenyl diluent(R1) with strong rigidity,it achieved excellent balance performance between room temperature/high temperature die shear force and residual adhesive rate.For aliphatic diglycidyl ether diluents(R2,R3) with good flexibility,their comprehensive performance was between the two.(3) The high-temperature steaming and moisture and heat aging test showed that the hydrophobic phenyl group in the diluent helped improve the moisture and heat resistance of die attach adhesive.

2025 年 06 期 v.34 ; 浙江省尖兵研发攻关计划项目(2023C01087)
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布敦岩复合改性沥青灌缝胶的制备与性能研究

Preparation and performance study of Buton rock composite modified asphalt grouting adhesive

王园明;赵苏; Wang Yuanming;Zhao Su;

本研究将布敦岩沥青与其他改性剂复合,制备了一种复合改性沥青灌缝胶。其中选用布敦岩沥青(BRA)、苯乙烯-丁二烯-苯乙烯嵌段共聚物(SBS)聚合物、橡胶粉、增容剂、增塑剂和增黏剂对基质沥青进行复合改性,采用6因素3水平正交试验设计,以路面灌缝胶的常规性能作为评价指标,通过极差分析法和方差分析法探究了各因素对灌缝胶性能的影响程度,研究布敦岩复合改性沥青灌缝胶的最佳配合比。通过布氏旋转黏度试验确定了灌缝胶的最佳施工温度,采用室内试验模拟评价了灌缝胶的储存老化性能,采用扫描电镜观察了灌缝胶与骨料界面的粘接情况。研究结果表明:通过正交试验极差分析和方差分析结果可知,布敦岩沥青和SBS对路面灌缝胶的常规性能均具有显著影响,布敦岩复合改性沥青灌缝胶满足路面灌缝胶技术指标要求(JT/T 740—2015)中高温型灌缝胶的要求。布敦岩沥青和SBS聚合物对于复合改性沥青灌缝胶的性能影响相比其他因素较大,布敦岩复合改性沥青灌缝胶的最佳配比(质量分数比)为,m(基质沥青)∶m(布敦岩沥青)∶m(SBS)∶m(废胶粉)∶m(增容剂)∶m(增塑剂)∶m(增黏剂)=100∶16∶8∶20∶10∶2∶2。布敦岩复合改性沥青灌缝胶的最佳施工温度为195.5℃,现场储存时间不应超过12 h。通过扫描电镜设备发现,布敦岩复合改性沥青灌缝胶与骨料界面的粘接性良好。

A composite modified asphalt grouting adhesive was prepared by combining Buton rock asphalt with other modifiers in this study. Among them,Buton rock asphalt(BRA),styrene-butadiene-styrene block copolymer(SBS) polymer,rubber powder,compatibilizer,plasticizer,and tackifier were selected for composite modification of matrix asphalt. A six-factor three-level orthogonal experimental design was adopted,and the conventional performance of pavement grouting adhesive was used as the evaluation index.The influence of various factors on the performance of grouting adhesive was explored through range analysis and variance analysis,and the optimal mixing ratio of Buton rock composite modified asphalt grouting adhesive was studied. The optimal construction temperature of the grouting adhesive was determined through the Brookfield rotational viscosity test.The storage aging performance of the grouting adhesive was evaluated through indoor test simulation.The bonding between the grouting adhesive and the aggregate interface was observed using scanning electron microscopy.The research results showed that through the analysis of range and variance in orthogonal experiment,it could be concluded that both Buton rock asphalt and SBS had a significant impact on the conventional performance of pavement grouting adhesive. Buton rock composite modified asphalt grouting adhesive met the technical requirements(JT/T 740—2015) for high temperature grouting adhesive. Compared with other factors,the performance of composite modified asphalt grouting adhesive was greatly affected by Buton rock asphalt and SBS polymer.The optimal ratio(mass fraction ratio) of Buton rock composite modified asphalt grouting adhesive was,m(matrix asphalt)∶m(Buton rock asphalt)∶m(SBS)∶m(waste rubber powder)∶m(compatibilizer)∶m(plasticizer)∶m(tackifier)=100∶16∶20∶10∶2∶2.The optimal construction temperature of grouting adhesive was 195.5 ℃,and the on-site storage time was ≤12 h.Through scanning electron microscopy equipment,it was found that the bonding between the Budun rock composite modified asphalt grouting adhesive and the aggregate interface was good.

2025 年 06 期 v.34 ;
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工艺与应用

加固用定向碳纤维板拉伸性能标准解析与测试方法探究

Analysis of tensile performance standards and testing methods for reinforced oriented carbon fiber plate

安绍都;马亚楠;张铭轩;姚淑芳;闫雨婷;闫新宇;曾兵; An Shaodu;Ma Yanan;Zhang Mingxuan;Yao Shufang;Yan Yuting;Yan Xinyu;Zeng Bing;

由环氧树脂浸润硬化形成的加固用定向碳纤维板是纤维增强复合材料中的一种关键材料,其拉伸性能对结构的安全性与耐久性有着重要的意义。本文比较和分析了国内外碳纤维板材相关标准的拉伸性能检测方法和技术指标,考察了对碳纤维板拉伸性能测试结果产生影响的因素,初步探索了不同厂家、不同厚度的碳纤维板拉伸性能检测数据,对有关碳纤维板的拉伸性能测试方法的检测技术进行了评价。

The reinforced oriented carbon fiber plate formed by infiltration hardening of epoxy resin is a key material in fiber reinforced composite materials,and its tensile performance is of great significance for the safety and durability of the structure. The tensile performance testing methods and technical indicators of carbon fiber plate related standards at home and abroad were compared and analyzed in this article,the factors that affected the tensile performance testing results of carbon fiber plate were investigated,the tensile performance testing data of carbon fiber plate with different thicknesses from different manufacturers were preliminarily explored,and the testing techniques related to the tensile performance testing methods of carbon fiber plate were evaluated.

2025 年 06 期 v.34 ; 建研院检测中心有限公司自筹青年科研基金资助(20220126977430005);建研院检测中心有限公司自筹科研基金项目(20220126977130006)
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